Le réseau
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L'organisation
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La structure de veille et de réflexion prospective
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Actualités
Le CERMAV développe des nanocristaux de cellulose à double fonction pour les émulsions et les revêtements biosourcés
Une collaboration associant le CERMAV à Grenoble montre que des nanocristaux de cellulose modifiés par des chaînes alkyles peuvent à la fois stabiliser des émulsions de Pickering et renforcer des revêtements biosourcés.
Les nanocristaux de cellulose constituent des nano-objets renouvelables particulièrement intéressants pour la formulation de matériaux. Leur forte rigidité et leur surface riche en fonctions hydroxyle permettent notamment de modifier finement leurs propriétés interfaciales afin de les utiliser comme agents de stabilisation ou comme renforts.
Dans ce travail, Sami Boufi, Fatma Ben Cheikh et Ayman Ben Mabrouk de l’Université de Sfax collaborent avec Jean-Luc Putaux, chercheur à l’Université Grenoble Alpes et au CNRS au sein du CERMAV. Les nanocristaux de cellulose sont fonctionnalisés par des chaînes octyle ou dodécyle au moyen d’une oxydation périodate suivie d’une amination réductrice. Cette modification permet d’ajuster leur équilibre hydrophile–hydrophobe tout en conservant une bonne dispersibilité dans l’eau.
Le greffage améliore fortement leur activité à l’interface huile-eau. Les nanocristaux modifiés produisent des émulsions de Pickering présentant des gouttelettes plus petites, une meilleure résistance à la coalescence et une stabilité accrue par rapport aux particules non modifiées. Ils renforcent également le caractère de gel des formulations, ce qui contribue à immobiliser les gouttelettes.
Les chercheurs démontrent ensuite leur utilisation dans une émulsion sans tensioactif à base d’huile de soja époxydée. Après réticulation, les nanocristaux ne jouent plus seulement le rôle d’émulsifiants : leur réseau rigide augmente aussi la rigidité du film obtenu. Cette double fonction ouvre des perspectives intéressantes pour la mise au point de formulations aqueuses et de revêtements biosourcés combinant stabilisation colloïdale et renforcement mécanique.
Publication : Effect of Alkyl Grafting on the Interfacial Properties and Pickering Emulsifying Efficiency of Cellulose Nanocrystals, ACS Omega.
L’ISIS de Strasbourg optimise la lecture de polymères numériques par nanopores biologiques
Jean-François Lutz, directeur de recherche au CNRS et responsable du Laboratoire de chimie des macromolécules informationnelles de l’Institut de science et d’ingénierie supramoléculaires, CNRS–Université de Strasbourg, participe à une étude consacrée au décodage de polymères synthétiques porteurs d’information. Une bibliothèque de polymères à séquence définie a été conçue afin d’étudier l’influence de l’hydrophilie, de la rigidité du squelette et de l’encombrement des unités sur leur passage dans un nanopore d’aérolysine. La combinaison d’un squelette cyclique rigide et d’unités latérales benzylées améliore la différenciation des signatures électriques. Associée à une classification par apprentissage automatique, cette conception moléculaire permet d’identifier des séquences atteignant 22 bits et renforce les perspectives de stockage moléculaire de données sur des polymères synthétiques.
https://onlinelibrary.wiley.com/doi/pdf/10.1002/ange.1446100
IUPAC MACRO 2028 : rendez-vous à Strasbourg !
À l’occasion de la clôture d’IUPAC MACRO 2026 (https://macro2026.org/image-gallery), le 51e World Polymer Congress organisé à Kuching en Malaisie, le relais a officiellement été passé à la France : la prochaine édition du congrès IUPAC MACRO se tiendra à Strasbourg du 28 au 31 août 2028.
MACRO 2028 sera présidé par Daniel Grande, Directeur de recherche au CNRS et directeur de l’Institut Charles Sadron (ICS, CNRS) à Strasbourg, en qualité de Chair, aux côtés de Delphine Chan-Seng, chercheuse CNRS à l’Institut Charles Sadron (ICS, CNRS), en qualité de Co-Chair. lire plus…
Des complexes de titane pour produire du polyéthylène de très haute masse molaire et ses copolymères
Deux complexes de titane(IV) basés sur un ligand tétradentate bis(phénolate)-pipérazine sont évalués pour la polymérisation de l’éthylène. Après activation par un système organoaluminium–organomagnésien, les catalyseurs produisent des polyéthylènes de très haute masse molaire et peuvent incorporer plusieurs alpha-oléfines, dont le 1-hexène, le 1-octène et le 1-décène. Les teneurs en comonomère peuvent dépasser 10 % molaires tout en conservant des masses molaires élevées. Le travail fournit une nouvelle famille de catalyseurs moléculaires pour ajuster conjointement architecture des chaînes et incorporation des comonomères.
SpringerLink Une nouvelle méthode cinétique pour analyser la fusion non isotherme des polymères
Une approche cinétique fondée sur les températures des pics de fusion enregistrées à différentes vitesses de chauffage permet d’extraire des informations sur la fusion sans imposer les approximations classiques de certaines analyses non isothermes. La méthode dérive d’une formulation exponentielle inspirée du modèle de Toda–Hikosaka–Yamada et a été validée par simulation puis appliquée au polyéthylène. Son comportement a ensuite été évalué sur plusieurs polymères semi-cristallins, notamment le polypropylène, le PCL, le PET, le PBT et le PVDF. Des scripts compatibles GNU Octave et MATLAB accompagnent l’approche afin de faciliter son utilisation pour la caractérisation thermique.
Nature Des déchets de pneus incorporés directement dans une matrice de polyéthylène recyclé
Des particules de caoutchouc provenant de pneus broyés sont dispersées dans une matrice de polyéthylène basse densité afin de produire des composites intégrant deux flux de déchets difficiles à valoriser. Les propriétés physiques, mécaniques et thermiques sont comparées pour différentes formulations, puis une méthode multicritère TOPSIS est utilisée pour sélectionner le compromis le plus favorable entre performances et contenu recyclé. L’approche vise des applications dans la construction, l’automobile et des composants industriels pour lesquels une rigidité maximale n’est pas le seul critère de choix.
SpringerLink Lorem ipsum dolor sit amet, consectetur adipiscing elit. Sed posuere tincidunt quam sit amet viverra. Nam in consequat nulla. Nunc rhoncus orci vitae arcu sagittis, in auctor nibh posuere. Donec ut nulla id enim tempor feugiat.
Adhérez au GFP
Devenez un membre et découvrez les avantages d’un abonnement GFP.
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Sections locales GFP
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Les partenaires
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lrccp
http://www.ispa.asso.fr
arkema
http://www.coatex.com
Logo-ChemSuD
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cnrs
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LPMC
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hutchinson
http://www.hutchinson.com/fr
logo-ispa_coul_fond-fonce
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http://www.waters.com
ICS
https://www-ics.u-strasbg.fr/
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