Le réseau
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L'organisation
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La structure de veille et de réflexion prospective
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Actualités
Prix GFP Thèse 2025 : Antoine Brézault
Antoine Brézault a réalisé sa thèse intitulée « Microgels supramoléculaires stimulables : du contrôle de la microstructure à l’étude de leur comportement aux interfaces » au Centre de Recherche Paul Pascal, en collaboration avec le Nsysa de l’ISM et le laboratoire Sciences et Ingénierie de la Matière Molle (SIMM) à Paris. Encadrée par Véronique Schmitt, Valérie Ravaine, Nicolas Sanson et Patrick Perrin, cette thèse a été financée par un Contrat Doctoral Spécial Normalien (CDSN) obtenu par Antoine. lire plus…
Valorisation sélective du polyéthylène par découplage-recouplage cinétique
Une équipe de recherche a élaboré une stratégie catalytique en tandem baptisée « découplage-recouplage cinétique » visant à transformer sélectivement les déchets de polyéthylène en monomères légers. Ce procédé novateur surmonte l’inertie chimique des liaisons carbone-carbone saturées en orchestrant deux cycles réactionnels distincts : une déshydrogénation initiale sur zéolithe générant des sites insaturés réactifs, suivie d’une scission contrôlée de la chaîne polymère par dimérisation et rupture bêta. L’ingéniosité du système réside dans la modulation précise des vitesses réactionnelles, permettant d’éviter l’accumulation d’intermédiaires stables qui entravent habituellement l’efficacité globale ou empoisonnent les catalyseurs. En favorisant la production exclusive de propylène et d’éthylène de haute pureté directement utilisables pour la repolymérisation, cette approche offre une voie thermochimique viable pour boucler le cycle de vie des plastiques polyoléfiniques, résolvant ainsi les défis de sélectivité inhérents aux méthodes de pyrolyse conventionnelles.
https://phys.org/news/2025-12-kinetic-decoupling-recoupling-strategy-enables.html
Initiation photothermique de la polymérisation frontale pour l’impression 3D de composites
Des chercheurs ont développé une stratégie d’initiation photothermique sans contact permettant de piloter la polymérisation frontale au cours de l’impression 3D de composites polymères. Ce procédé exploite la capacité des renforts en fibres de carbone à absorber l’énergie d’un faisceau laser pour générer localement la chaleur nécessaire au démarrage d’une réaction de durcissement auto-entretenue. En s’affranchissant des sources de chaleur externes globales ou des contacts physiques limitants, cette méthode assure une solidification quasi instantanée de la résine thermodurcissable dès sa dépose, facilitant la fabrication de formes libres sans outillage complexe. Cette innovation améliore considérablement l’efficacité énergétique et la vitesse de production par rapport aux cycles de cuisson conventionnels, tout en préservant l’intégrité structurelle des pièces. Elle présente un potentiel industriel majeur pour l’élaboration automatisée et continue de matériaux composites à haute performance, notamment pour des applications nécessitant une grande liberté de conception ou des interventions de réparation rapide.
Nature Hydrogels biomimétiques anisotropes à haute ténacité par nanocristallisation progressive
Des chercheurs ont développé une stratégie de fabrication séquentielle pour élaborer des hydrogels mimétiques de tissus biologiques présentant une résistance exceptionnelle à la propagation des fissures. Cette approche innovante repose sur la nanocristallisation progressive de réseaux polymères anisotropes, obtenue par la combinaison synergique d’un entraînement mécanique, d’un recuit humide et d’un processus de relargage salin. Ce protocole permet d’orienter les chaînes moléculaires et d’induire la formation contrôlée de domaines cristallins à plusieurs échelles, créant ainsi une architecture hiérarchique dense similaire à celle des structures biologiques naturelles comme les tendons ou les muscles. Les matériaux résultants surmontent les compromis habituels entre rigidité et extensibilité, offrant une durabilité et une tolérance aux défauts nettement supérieures aux hydrogels synthétiques conventionnels. Cette maîtrise fine de la microstructure et de l’anisotropie ouvre des perspectives technologiques majeures pour la conception d’implants biomédicaux sous contrainte, de dispositifs de robotique souple et de matériaux de remplacement pour l’ingénierie tissulaire avancée.
Nature Caractérisation multimodale dynamique des hydrogels thermo-sensibles sous contrainte
Des chercheurs ont mis au point un dispositif analytique hybride combinant la rhéométrie et la spectroscopie d’impédance électrochimique pour élucider le comportement interne des gels de poly(N-isopropylacrylamide) soumis simultanément à des contraintes de cisaillement et des variations thermiques. Cette technique de « rhéo-impédance » permet de capturer en temps réel les modifications de la microstructure du réseau polymère sans perturber son intégrité physique. L’étude démontre que lors de la transition de phase volumique, le matériau passe d’un état hydraté et conducteur à une configuration déshydratée hétérogène, où la formation de domaines hydrophobes agit comme des barrières isolantes limitant la mobilité ionique. En corrélant ces variations de conductivité et de capacitance avec les changements de rigidité mécanique, validés par diffusion des rayons X aux petits angles, l’équipe a établi une méthodologie robuste pour surveiller l’évolution structurale des matériaux intelligents. Cette avancée instrumentale offre des perspectives cruciales pour l’ingénierie de dispositifs adaptatifs, tels que les actionneurs pour la robotique molle, les capteurs flexibles et les vecteurs de délivrance de médicaments, nécessitant un contrôle précis de leurs propriétés physico-chimiques en conditions réelles d’utilisation.
https://phys.org/news/2025-12-smart-gels-scientists-capture-dynamic.html
Polymères autodestructibles robustes régulés par nanoconfinement de liaisons hydrogène
Une innovation récente démontre que l’ingénierie macromoléculaire permet de concevoir une nouvelle classe de polymères capables d’allier une robustesse mécanique exceptionnelle à une autodestruction programmable déclenchée par l’humidité ambiante. Ces matériaux, élaborés via une synthèse en milieu aqueux reposant sur la réaction d’Aza-Michael, se distinguent par une architecture interne singulière où des liaisons hydrogène à haute densité s’organisent en nanogroupes confinés ordonnés. Cette structure hiérarchique, inspirée biomimétiquement de la soie d’araignée, confère au matériau une rigidité élevée à l’état sec en minimisant l’enchevêtrement des chaînes, tout en conservant une sensibilité hygroscopique intrinsèque grâce à l’abondance de groupes hydrophiles. L’exposition à l’humidité provoque l’absorption spontanée de molécules d’eau qui perturbent l’équilibre des nanogroupes, entraînant une transition de phase physique réversible du solide vers un fluide viscoélastique. Ce mécanisme de déconstruction, dont la cinétique est modulable par la composition chimique et les conditions environnementales, offre une voie prometteuse pour le développement de dispositifs transitoires. Les applications potentielles de cette technologie s’étendent des structures temporaires porteuses aux vecteurs autodestructibles, en passant par l’électronique transitoire et la réduction des déchets technologiques, répondant ainsi aux besoins croissants de matériaux à cycle de vie contrôlé sans nécessiter de stimuli énergétiques complexes ni de solvants spécifiques.
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Les partenaires
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hutchinson
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LPMC
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ICS
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http://www.waters.com
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