Le réseau
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L'organisation
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La structure de veille et de réflexion prospective
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Actualités
Des enchevêtrements moléculaires pour régénérer des thermodurcissables techniques
Une analyse publiée dans Nature Materials présente une stratégie associant une forte densité d’enchevêtrements physiques à une faible proportion de jonctions covalentes clivables. Les enchevêtrements assurent l’essentiel des propriétés mécaniques, tandis que les réticulations maintiennent temporairement la cohésion du réseau. Leur rupture contrôlée libère des chaînes pouvant être remises en solution, reformées puis réticulées. Cette conception cherche à concilier les performances des thermodurcissables techniques avec plusieurs cycles de régénération.
Nature La biomasse de sargasses est transformée par calcination en une charge minérale destinée à des composites de polypropylène recyclé. Un traitement de surface par agent de couplage silane améliore la compatibilité entre les particules minérales et la matrice polymère. Les auteurs examinent les propriétés mécaniques, thermiques et fonctionnelles des formulations obtenues. La démarche combine la gestion d’une biomasse marine envahissante, la valorisation d’une ressource minérale et l’emploi d’une matrice issue du recyclage.
SpringerLink Origine électronique de l’adhésion chimique aux interfaces métal-polymère
En combinant calculs de structure électronique et caractérisations expérimentales, les chercheurs proposent un modèle unifié des interactions donneur-accepteur aux interfaces métal-polymère. Les oxydes métalliques de surface et les groupes carboxyle du polymère favorisent la formation de coordinations pontantes entre les deux matériaux. La création de lacunes d’oxygène renforce la capacité des sites métalliques à accepter des électrons et stabilise l’interface. Le mécanisme a été étudié sur plusieurs alliages, états de valence et polymères thermoplastiques, avec une amélioration de la résistance au cisaillement supérieure à 400 % dans le système optimisé.
L’eau transformée en réticulateur cinétique pour des polymères se rigidifiant sous impact
Habituellement considérée comme un plastifiant indésirable, l’eau résiduelle devient ici un composant actif du réseau polymère. Confinées dans une matrice riche en protons, les molécules d’eau forment un réseau dynamique de liaisons hydrogène dont la dissociation dépend de la vitesse de sollicitation. Sous impact, le matériau passe rapidement d’un état souple à un état rigide, tout en conservant des capacités d’auto-réparation, d’adhésion et de dissipation d’énergie. Le principe, démontré avec le poly(acide thioctique), peut être étendu à d’autres polymères hydrophiles riches en fonctions acides.
La répartition des additifs gouverne la dégradation des plastiques exposés à l’environnement
Une collaboration associant notamment Géosciences Rennes, l’Institut de physique de Rennes, l’Institut des sciences chimiques de Rennes, le Synchrotron SOLEIL, ISTerre et INRAE montre que la dégradation de fragments de polyéthylène dépend fortement de l’organisation spatiale initiale de leurs additifs. La microfluorescence X synchrotron et la spectroscopie infrarouge photothermique révèlent trois comportements distincts : rupture préférentielle des domaines riches en additifs, redistribution des éléments le long des fissures oxydées et altération plus homogène des formulations faiblement structurées. La proximité du titane et du chrome avec les fronts d’oxydation souligne que la topologie des additifs constitue un paramètre déterminant, indépendamment de leur concentration globale.
Pyrolyse à basse température de polyuréthanes sans isocyanate
L’article analyse la transformation thermique de polyuréthanes sans isocyanate au moyen de techniques thermo-analytiques couplées et d’une étude cinétique détaillée. Les profils de décomposition permettent d’identifier les différentes étapes de rupture de la structure macromoléculaire et de relier leur progression à la température et à la composition du matériau. Ce travail fournit une base expérimentale pour concevoir des procédés de pyrolyse à basse température adaptés au recyclage chimique de cette famille de polyuréthanes.
https://www.sciencedirect.com/science/article/pii/S004060312600184X
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Adhérez au GFP
Devenez un membre et découvrez les avantages d’un abonnement GFP.
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Sections locales GFP
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